Sintesis senyawa risinoleil dietanolamida melalui reaksi amidasi asam risinoleat dengan dietanolamina

Amalia, Suci (2012) Sintesis senyawa risinoleil dietanolamida melalui reaksi amidasi asam risinoleat dengan dietanolamina. sainstis, 1 (1). ISSN ISSN: 2089-0699

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Abstract

There was a synthesis of derived amida of risinoleat acid compound through amidasi reaction. Risinoleat Acid obtained through metil risinoleat isolation from jarak oil through trans-esterifikasi reaction using natrium metoksida, and then doing hidrolisis metil risinoleat. Amidasi reaction to risinoleat acid was obtained by adding dietanolamina to the high temperature during 6 hours. Structure confirmation from the result compound is characterized by spektrometer IR and GC-MS.

Amidasi risinoleat acid reaction and dietanolamina produce risinoleil dieanolamida compound as like thick liquid, chocolate yellowness coloured with rendemen 45,26 %. The lost of acid karbonil cluster absorption from analysis IR result to alkanolamida compound cannot convince that amida compound is 100% formed.

Item Type: Journal Article
Keywords: risinoleat acid; dietanolamina; amidasi reaction; jarak oil
Subjects: 03 CHEMICAL SCIENCES > 0305 Organic Chemistry > 030503 Organic Chemical Synthesis
Divisions: Faculty of Mathematics and Sciences > Department of Chemistry
Depositing User: Mrs Suci Amalia
Date Deposited: 24 Sep 2019 20:12

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